Synephrine 94-07-5 Manufacturer Exporter Supplier MEDIOCON INC

 

 

Synephrine Manufactured by MEDIOCON INC     

 

   Name: Synephrine

CAS No:  94-07-5

Molecular Weight: 167.21g/mol

Molecular formula:   C9H13NO2

Synonyms p-Synephrine; Oxedrine; 4, β-Dihydroxy-N-methylphenethylamine

Appearance colorless crystalline Solid.

 Solubility :  Soluble in water

Use :

Synephrine is a multifaceted compound with various uses, ranging from medical applications to weight loss and sports performance enhancement. Here are some of its primary uses:

- Medical Applications

    - Decongestant: Synephrine is used to relieve nasal congestion caused by colds and hay fever, with noticeable effects within 15-30 minutes.

    - Pupil Dilation: Ophthalmic formulations of synephrine are used to dilate pupils during eye exams or surgeries.

    - Hypotension Treatment: Synephrine injections help treat low blood pressure caused by shock or anesthesia.

    - Hemorrhoid Relief: Topical formulations provide relief from hemorrhoid symptoms.

- Weight Loss and Sports Performance

    - Fat Burning: Synephrine increases thermogenesis, helping the body burn more calories and fat, which can aid in weight loss.

    - Energy Enhancement: It provides more energy for physical activities, making it popular among athletes and individuals seeking to improve their workout performance.

    - Appetite Suppression: Synephrine may help reduce appetite, supporting weight loss efforts.

- Other Potential Benefits

    - Anti-Inflammatory Effects: Synephrine has shown promise in reducing inflammation and oxidative stress.

    - Antimicrobial Properties: Laboratory studies suggest synephrine may inhibit the growth of certain bacteria and fungi.

    - Improved Concentration: Some users report enhanced mental performance and focus when taking synephrine.

 How is  Synephrine manufactured by MEDIOCON INC Synthesized?

Synephrine can be synthesized through various methods, including:

 

- Chemical Synthesis: One method involves reacting phenol with acetyl chloride or diacetyl oxide to produce phenol acetate, which then undergoes Friedel-Crafts rearrangement, bromination, amination, and reduction to form synephrine.

- Hoesch Acylation Reaction: Another method uses phenol as the main raw material, reacting it with N-methylamino acetonitrile hydrochloride in the presence of a Lewis acid catalyst to generate corresponding ketimine, which is then hydrolyzed to obtain 1-(4-hydroxyphenyl)-2-(methylamino) acetophenone hydrochloride. This intermediate is then reduced through Pd/C catalytic hydrogenation to produce synephrine hydrochloride.

- Plant-Based Synthesis: Synephrine is also naturally produced in certain plants, such as Citrus aurantium, through a biosynthetic pathway involving tyrosine, tyramine, and N-methyltyramine.

- Derivative Synthesis: Researchers have also synthesized synephrine derivatives, such as 2-(hexylamino)-1-(4-nitrophenyl)ethanol, which have shown potential anti-cancer activity.¹ ²

The synthesized synephrine can be further processed to obtain its hydrochloride or tartrate forms, which have various applications in pharmaceuticals and dietary supplements.

What are the different  dosage forms  of   Synephrine Manufactured  by  MEDIOCON INC?

Synephrine dosage forms vary depending on the intended use and product formulation. Here are some common dosage forms and their corresponding dosages:

- Weight Loss and Energy Enhancement

    - Typical Dosage: 4-20 mg of synephrine per day, often found in standardized citrus aurantium extract supplements (200-600 mg per pill, containing 3-6% synephrine).

    - Effective Dosage: 10-53 mg of synephrine per day has been shown to be effective for weight management.

- Athletic Performance

    - Acute Intake: 100-200 mg of bitter orange extract (containing synephrine) taken before exercise may enhance athletic performance.

- Other Forms

    - Injection: Synephrine injections are used to treat hypotension caused by shock or anesthesia.

    - Ophthalmic Formulation: Used to dilate pupils and induce vasoconstriction.

    - Intranasal Formulation: Used to treat nasal congestion.

    - Topical Formulation: Used to relieve hemorrhoids.

It's essential to follow the manufacturer's dosage guidelines and consult with a healthcare professional before taking synephrine supplements, especially if you have pre-existing health conditions or take medications.

 How Synephrine Manufactured by MEDIOCON INC   Dosage Forms are prepared?

Synephrine dosage forms are prepared in various ways depending on the intended use and product formulation. Here are some common preparations:

 

- Injection Preparation: For intravenous or intramuscular use, synephrine (phenylephrine hydrochloride) is typically diluted with a compatible infusion fluid, such as sodium chloride 0.9% or dextrose 5%. The usual preparation involves adding 10mg of phenylephrine (1mL of 10mg/mL solution) to 100mL of infusion fluid, resulting in a 100 microgram/mL solution.

- Rectal Preparation: For hemorrhoid treatment, synephrine is often combined with other ingredients like pramoxine, glycerin, and petrolatum. The rectal ointment or cream typically contains 0.25% phenylephrine hydrochloride, and is applied externally to the affected area up to 4 times daily.

- Dosage Forms: Synephrine is available in various dosage forms, including¹ ² ³:

    - Injectable Solution: 10mg/mL ampoule, diluted before administration

    - Rectal Ointment/Cream: 0.25% phenylephrine hydrochloride, often combined with pramoxine and other ingredients

    - Tablets/Liquid: Available in various concentrations, often used for weight loss and athletic performance

 

It's essential to follow the manufacturer's instructions and consult with a healthcare professional before using synephrine products, especially if you have pre-existing health conditions or take medications.

What are the appropriate Dosage forms of Synephrine Manufactured  by  MEDIOCON   INC?                

The appropriate dosage forms of synephrine vary depending on the intended use and individual factors. Here are some general guidelines:

 

- Weight Loss and Energy Enhancement:

    - Typical Dosage: 4-20 mg of synephrine per day, often found in standardized citrus aurantium extract supplements (200-600 mg per pill, containing 3-6% synephrine).

    - Effective Dosage: 10-53 mg daily doses have been shown to be effective for weight management.

- Athletic Performance:

    - Acute Intake: 100-200 mg of bitter orange extract (containing synephrine) taken before exercise may enhance athletic performance.

- Recommended Dosage: Some studies suggest¹ ² ³:

    - 30-50 mg: A recommended dosage range for safe and effective use.

    - 50 mg: Shown to increase resting metabolic rate without increasing blood pressure.

    - Up to 100 mg: Considered safe with no significant cardiovascular effects.

It's essential to follow the manufacturer's dosage guidelines and consult with a healthcare professional before taking synephrine supplements, especially if you have pre-existing health conditions or take medications.

When should Synephrine Manufactured by MEDIOCON INC be taken?

The timing of synephrine intake depends on the intended use and individual factors. Here are some general guidelines:

- Weight Loss and Energy Enhancement:

    - Before Meals: Taking synephrine 30-60 minutes before meals may help reduce appetite and increase fat burning.

    - In the Morning: Taking synephrine in the morning may help boost energy and metabolism throughout the day.

- Athletic Performance:

    - Before Exercise: Taking 100-200 mg of bitter orange extract (containing synephrine) 30-60 minutes before exercise may enhance athletic performance.

- General Guidelines:

    - Start with a Low Dose: Begin with a low dose and gradually increase as needed and under medical supervision.

    - Avoid Taking Before Bedtime: Synephrine can interfere with sleep due to its stimulating effects.

    - Consult a Healthcare Professional: Before taking synephrine, especially if you have pre-existing health conditions or take medications

 What are the effects And Side effects of Synephrine Manufactured by MEDIOCON INC?

Synephrine is a natural stimulant found in citrus fruits, particularly bitter oranges, that offers several benefits, including weight loss and enhanced physical performance. However, its use can also lead to various side effects.

 

Positive Effects:

 

- Weight Loss: Synephrine supports fat burning while providing energy, making it useful for demanding physical activities and weight management.

- Improved Concentration: It can contribute to improved mental performance and focus.

- Metabolism Boost: Synephrine increases thermogenesis, helping the body burn more calories and fat.

- Mild Appetite Suppressant: It can help reduce excessive calorie intake.

 

Side Effects:

 

- Cardiovascular Issues: Increased heart rate and blood pressure, potentially leading to heart palpitations, tachycardia, and heart arrhythmia.

- Neurological Effects: Anxiety, jitteriness, insomnia, and headaches due to its stimulatory effect on the nervous system.

- Gastrointestinal Issues: Nausea, vomiting, abdominal pain, and stomach upset, particularly when consumed on an empty stomach.

- Interactions with Medications: Synephrine may interact with certain medications, such as MAOIs, blood pressure medications, and stimulants, increasing the risk of adverse effects.¹ ² ³

Precautions:

- High Blood Pressure and Heart Conditions: Individuals with these conditions should consult a doctor before using synephrine.

- Pregnancy and Breastfeeding: The safety of synephrine during these periods is not well-established, so it's best to avoid its use unless advised by a healthcare professional.

- Combining with Other Stimulants: Avoid combining synephrine with other stimulants like caffeine, as it may increase the risk of adverse effects.

  How is Synephrine Manufactured by MEDIOCON  INC  Tested Qualitatively?

Synephrine can be tested qualitatively using various methods, including:

- High-Performance Liquid Chromatography (HPLC): This method is used to separate, identify, and quantify synephrine in a mixture. It's often coupled with mass spectrometry (MS) or diode-array detection for enhanced sensitivity and specificity.

- Liquid Chromatography-High Resolution Accurate Mass Mass Spectrometry (LC-HRAM-MS/MS): This technique evaluates matrix effects and provides accurate quantification of synephrine.

- Targeted LC-HRAM-MS/MS: This method is used for the detection and quantification of synephrine in various samples.

 

These methods are commonly used for¹ ² ³:

- Dietary Supplement Quality Control: To ensure the presence and accuracy of synephrine labeling.

- Food Adulteration Identification: To detect synephrine in food products.

- Pharmaceutical Analysis: To quantify synephrine in pharmaceutical preparations.

Researchers have also used these methods to analyze synephrine in various samples, including⁴ ⁵:

- Citrus Fruits and Products: To determine synephrine levels in different citrus species and products.

- Nutritional Supplements: To detect synephrine and other stimulants in nutritional supplements.

   Which tests are performed on Synephrine Manufactured by  MEDIOCON INC ?

Tests performed on synephrine include:

- High-Performance Liquid Chromatography (HPLC): To separate, identify, and quantify synephrine in a mixture.

- Liquid Chromatography-High Resolution Accurate Mass Mass Spectrometry (LC-HRAM-MS/MS): To evaluate matrix effects and provide accurate quantification of synephrine.

- Targeted LC-HRAM-MS/MS: For detection and quantification of synephrine in various samples.

- Tail Suspension Test: To assess antidepressant-like effects of synephrine in mice.

- Reserpine-Induced Hypothermia: To evaluate the antidepressant effects of synephrine.

- Forced Swimming Test: To assess antidepressant-like effects of synephrine in mice.

- Binding Experiments: To study the binding of synephrine to adrenergic receptors.

- Vasoconstriction Assays: To evaluate the effects of synephrine on blood vessels.

- Lipolysis Assays: To assess the lipolytic effects of synephrine on fat cells.

These tests help researchers understand synephrine's pharmacological effects, potential therapeutic applications, and safety profile.

What are the challenges in Manufacturing of Synephrine Manufactured by MEDIOCON   INC API?

The challenges in manufacturing Synephrine API are similar to those faced in the production of other Active Pharmaceutical Ingredients (APIs). Some of the key challenges include¹ ² ³:

- Regulatory Compliance: Synephrine manufacturers must comply with stringent regulations set by regulatory agencies like the FDA and EMA, ensuring consistency, safety, and efficacy of the API. This requires robust quality management systems, thorough documentation, and adherence to Good Manufacturing Practices (GMP).

- Complex Chemistry: The synthesis of Synephrine involves complex chemical reactions and processes, requiring a deep understanding of chemical reactions, process optimization, and impurity control.

- Impurity Control and Profiling: Identifying, minimizing, and consistently controlling impurities is crucial to ensure product quality and prevent regulatory setbacks. Advanced analytical methods like HPLC, LC-MS, and NMR are used to detect trace impurities.

- Yield Optimization: Achieving high yields while maintaining product quality is essential for cost-effective production. This can be achieved through process optimization, reaction kinetics, and real-time monitoring.

- Supply Chain Management: Synephrine manufacturers rely on a network of suppliers for raw materials, solvents, and reagents. Disruptions in the supply chain can lead to production delays and quality issues, making it essential to build strong relationships with reliable suppliers.

- Environmental Sustainability: The manufacturing process of Synephrine can have a significant environmental impact due to the use of chemicals, solvents, and energy-intensive processes. Adopting green chemistry principles and sustainable practices can help reduce the environmental footprint.

- Technology Transfer: Transferring the manufacturing process from laboratory to industrial scale poses technical and logistical hurdles. Detailed batch records, SOPs, and pilot-scale runs can help streamline this process.

- Cost-Efficiency and Scalability: Synephrine manufacturers need to balance production costs with quality and regulatory requirements. This can be achieved by optimizing synthetic routes, recycling solvents, and benchmarking costs.

- Quality Control and Assurance: Maintaining high-quality standards throughout the manufacturing process is essential to ensure the safety and efficacy of Synephrine. This requires robust quality control systems, thorough testing, and documentation.

By understanding and addressing these challenges, manufacturers can ensure the production of high-quality Synephrine API that meets regulatory standards and customer expectations.

What are the challenges in manufacturing of Synephrine Manufactured by MEDIOCON  INC ’s Dosage forms?

Manufacturing synephrine dosage forms poses several challenges, including:

- Regulatory Compliance: Ensuring consistency, safety, and efficacy of the dosage form while adhering to Good Manufacturing Practices (GMP) and regulatory guidelines.

- Complex Formulation: Synephrine's hygroscopic nature can lead to clumping, making it challenging to work with in various formulations.

- Stability Issues: Maintaining the stability of synephrine in dosage forms, particularly in liquid formulations, can be difficult due to chemical and physical changes over time.

- Product Uniformity: Ensuring uniform distribution of synephrine in solid dosage forms, such as tablets or capsules, can be a challenge, especially with low-dose formulations.

- Scalability: Scaling up synephrine dosage form manufacturing while maintaining consistency and quality can be a hurdle.

- Supply Chain Management: Managing raw material sourcing, manufacturing, and distribution can be complex, especially with potential supply chain disruptions.

- Technological Advancements: Adopting new technologies, such as 3D printing, can be challenging due to regulatory uncertainty and the need for specialized expertise.

- Patient-Centric Design: Designing dosage forms that meet patient needs, such as ease of administration and minimal side effects, can be a challenge.

- Quality Control: Ensuring the quality of synephrine dosage forms through rigorous testing and quality control measures is crucial to prevent defects and ensure safety.¹ ² ³

 

To overcome these challenges, manufacturers can adopt strategies such as⁴ ⁵:

- Process Optimization: Optimizing manufacturing processes to improve efficiency, reduce costs, and ensure consistency.

- Robust Quality Control: Implementing robust quality control measures to detect defects and ensure product quality.

- Supply Chain Resilience: Building resilient supply chains to mitigate disruptions and ensure consistent raw material sourcing.

- Technological Innovation: Adopting new technologies, such as continuous manufacturing and 3D printing, to improve efficiency and product quality.

What is the Packing for Synephrine Manufactured by MEDIOCON INC?

Synephrine packing typically refers to nasal packing procedures where Neo-Synephrine (phenylephrine) is used. Here's what you need to know:

 

Types of Packing- Nasal Packing: Used to control nosebleeds (epistaxis) by applying pressure to the bleeding site.

- Neo-Synephrine Soaked Cotton Ball: Sometimes used in nasal packing procedures to help reduce bleeding due to its vasoconstrictive properties.

 

Purpose- Control Bleeding: The primary goal of nasal packing with Neo-Synephrine is to stop bleeding by constricting blood vessels and applying pressure to the bleeding site.

- Reduce Swelling: Neo-Synephrine helps reduce swelling in the nasal passages, making it easier to manage bleeding.

 

Precautions- Avoid Blowing Nose: After nasal packing removal, avoid blowing your nose for at least 2 days to prevent re-bleeding.

- Follow Doctor's Instructions: Always follow your doctor's advice regarding nasal packing and aftercare.¹ ²

Product Availability- Neo-Synephrine Nasal Spray: Available over-the-counter in various strengths, including extra strength formulas.

What is shelf life Of Synephrine Manufactured by MEDIOCON INC? 

Synephrine's shelf life typically ranges from 2 to 3 years, depending on storage conditions and the specific product formulation. Here are some general guidelines:

- Standard Synephrine Powder: 2 years when sealed and stored away from direct sunlight

- Citrus Aurantium Extract (Synephrine): 2 years when expertly vacuum-packed in durable drums

- Synephrine HCl Powder: 36 months when stored in a cool, dry place

- Raw Synephrine Powder: 2 years when stored properly

To maximize shelf life, it's essential to¹ ² ³:

- Store synephrine in a cool, dry place with temperatures between 15-25°C (59-77°F)

- Keep it away from direct sunlight and moisture

- Use airtight containers made of materials like glass or high-density polyethylene (HDPE)

- Add silica gel packets or moisture-absorbing agents to maintain a low-humidity environment

Proper storage and handling can help preserve synephrine's potency and effectiveness throughout its shelf life.

What should the label claim for Synephrine Manufactured by MEDIOCON INC   Include?

The label claim for Synephrine should include the following information:

- Product Name and Description: Clearly state the product name and description, including the ingredient name (Synephrine) and its source (e.g., Citrus aurantium).

- Concentration and Amount: Specify the concentration of Synephrine per serving and the total amount per container.

- Serving Size and Directions: Provide serving size instructions and recommended usage guidelines.

- Warning and Precautions: Include warnings and precautions for use, such as potential interactions with medications or health conditions.

- Ingredient List: List all ingredients used in the product, including any fillers, binders, or other additives.

- Manufacturer Information: Provide the manufacturer's name, address, and contact information.

- Net Weight or Quantity: State the net weight or quantity of the product.

- Storage and Handling Instructions: Offer storage and handling instructions to maintain product stability and potency.

- Expiration Date or Shelf Life: Include an expiration date or shelf life to ensure product freshness and potency.

- Regulatory Compliance: Ensure compliance with relevant regulatory requirements, such as Good Manufacturing Practices (GMP) and labeling regulations [1][2][3].

By including this information, the label claim for Synephrine can provide transparency and help consumers make informed decisions about their use of the product.

Where can Synephrine Manufactured by MEDIOCON INC are procured?

Synephrine Manufactured by MEDIOCON INC   can be procured from various sources, depending on your location and requirements. Here are some options:

FOR API

MEDIOCON INC

Add: B-2, ARCH SARTHAK BUILDING, N-7 CIDCO

CHATRAPATI SAMBHAJI NAGAR-431003, MAHARASHTRA, INDIA

Mob/Whatsapp No: +91-8007719681, +91-9309999757, +91-9834786939

Sales Department: Email: sales@mediocon.com

Purchase Department: Email: purchase@mediocon.com

Marketing Department: Email: mktg@mediocon.com

HR Department: Email: hr@mediocon.com

Accounts Department: Email: accounts@mediocon.com          

Factory Address: Plot No 11, Shendra MIDC, Aurangabad-431154, Maharashtra, India Website:  www.mediocon.com 

Email id:info@mediocon.com           

GST No: 27DHUPM2366D1ZZ

For Dosage Forms :

- Online Marketplaces: You can find Synephrine Manufactured by MEDIOCON INC   products on online marketplaces like Amazon or e- commerce websites specializing in pharmaceuticals or skincare products.

Local Pharmacies or Skincare Stores: You can also check with local pharmacies or skincare stores in your area for Synephrine Manufactured by MEDIOCON INC products.

Remember to ensure the quality and authenticity of the Synephrine Manufactured by MEDIOCON INC product, regardless of the procurement source.

 

 

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